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LOOK Project

RESEARCH GROUPS

Research Group: Analytical Chemistry – BC

Scientists

Research Group Leader: Michał Kubecki, PhD tel. +48 (32) 23 45 251, e-mail: michal.kubecki@imz.lukasiewicz.gov.pl

Marta Kubiczek, PhD
Waldemar Spiewok, PhD
Aleksandra Zassowska, PhD
Edyta Klima, MSc
Piotr Knapik, MSc
Aleksandra Kwoka, MSc
Aleksandra Latacz, MSc
Alicja Ryczko, MSc
Anna Kaleta
Monika Żurawska

Equipment

Vacuum spectrometer (750 mm), equipped with spark excitation source, using digital setting of current parameters, with the possibility of spark recording.

Gas Chromatograph with mass spectrometer used for qualitative and quantitative analysis of organic compounds (PAH BTEX, PCB, PCDD, PCDF, PBB, PBDE).

Spectrometer with direct current (dc) power source as well as rf source for testing of non- conductive coatings and analytical channels for the following elements: H, N, O, C, Mn, Si, P, S, Cr, Mo, Ni, Al, B, Co, Cu, Nb, Ti, V, W, Fe, As, Pb, Cd, Sn, Sb Zr, Ca, Zn, Ce, Ta, Hf, Pt, Re, Pd, Y.

Optical emission spectrometer with excitation in an inductively coupled plasma with Echelle optics, is equipped with source of vertical plasma and peripheral device for hydride analysis.

The spectrometer is equipped with an X-ray lamp with Rh anode, 4,0 kW power, with front Be window, thickness: 30 microns. Set of 7 analysing crystals (LiF200, LiF220, PET, Ge and 3 multi-layer crystals) facilitates qualitative and quantitative analysis of elements ranging from carbon to uranium.

Sequence spectrometer with 1m optics, equipped with vertical plasma source and supplementary device for analysis of hydrides. The spectrometer is also used for analysis of samples (sorting) from the perspective of compliance with directive RoHS 2002/95/WE.

The spectrometer with atomization in graphite cell used for determining Au, Ag, As, Bi, Cu, Mn, Pb, Se, Sn, Sb, Te, Tl i Y.

Research stand for tests of examinations of decomposition of materials used in foundry (binding agents, hardening agents, reclaims) facilitates examination of the impact of temperature ranging from 100^oC – 1300^oC on type and number of organic compounds (PAH, BTEX) released during thermal decomposition of selected materials.

The analyzer is used for determination of mercury content in solid, liquid and gaseous materials.

The analyzer is used for simultaneous determination of the content of oxygen, nitrogen and hydrogen in steels, cast iron, nickel, cobalt, titanium, copper alloys as well as content of nitrogen in ferroalloys.

The analyzer is used for determining carbon and sulphur content in metallic materials (steel, cast iron, iron alloys, nickel alloys, cobalt alloys, titanium alloys aluminum and copper alloys), in slags and ores.

Laboratory performs determination of the content of elements by means of classical methods (weighing and titration as well as spectrophotometric) as well as prepares samples of isolates and solutions for instrumental methods analyses: GF AAS and OES ICP.

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TABLE OF CONTENTS

PUBLISHING

Jarosław MARCISZ, Józef PADUCH, Adam ZIELIŃSKI

ŁUKASIEWICZ RESEARCH NETWORK – INSTITUTE FOR FERROUS METALLURGY – CURRENT AND FUTURE RESEARCH ACTIVITIES

Marek BURDEK, Bogdan GARBARZ, Dariusz WOŹNIAK, Mariusz ADAMCZYK, Jacek SKIBA, Mariusz KULCZYK

UNCONVENTIONAL METHODS OF MANUFACTURING THIN WIRES FOR APPLICATION AS INPUT MATERIAL IN ADDITIVE MANUFACTURING. PART 1: PREPARATION OF INPUT MATERIAL FOR WIRE DRAWING

Marek BURDEK, Mariusz ADAMCZYK, Krzysztof MARSZOWSKI

UNCONVENTIONAL METHODS OF MANUFACTURING THIN WIRES FOR APPLICATION AS INPUT MATERIAL IN ADDITIVE MANUFACTURING. PART 2: DRAWING OF Fe-BASED ALLOY WIRES

Marcin KEMPNY

DIGITAL IMAGE CORRELATION – METHOD DEVELOPMENT, SCOPE, PRINCIPLE OF FUNCTIONING, AND FUTURE GOALS

Hanna PURZYŃSKA , Grzegorz GOLAŃSKI

INCOLOY 800HT IRON-BASED SUPERALLOY – PRELIMINARY CHARACTERISATION

Piotr RÓŻAŃSKI, Mariusz BORECKI, Marian NIESLER, Janusz STECKO, Wojciech SZULC, Bogdan ZDONEK

DECARBONISATION PATHWAYS OF THE STEEL INDUSTRY

Ireneusz SZYPUŁA, Piotr RÓŻAŃSKI, Janusz STECKO, Marian NIESLER

DETERMINATION OF CONDITIONS FOR MAXIMUM DEZINCIFICATION OF A MIXTURE OF FERROUS MATERIALS IN THE SINTERING PROCESS BASED ON NUMERICAL CALCULATIONS USING THE FactSage THERMOCHEMICAL PROGRAM

SEE THIS ISSUE ARCHIVE

BIP IMZ

ESSA

Bioglass

Green Steel

LOOK-mod

PEDMO

PPTS

Marka POLSKA